6-Methoxylepidine
6-METHOXY-4-METHYLQUINOLINE
CAS: 41037-26-7
Molecular Formula: C11H11NO
6-Methoxylepidine - Names and Identifiers
6-Methoxylepidine - Physico-chemical Properties
| Molecular Formula | C11H11NO |
| Molar Mass | 173.21 |
| Density | 1.102±0.06 g/cm3(Predicted) |
| Melting Point | 53°C |
| Boling Point | 158 °C / 10mmHg |
| pKa | 5.69±0.16(Predicted) |
| Storage Condition | Sealed in dry,Room Temperature |
| MDL | MFCD00191547 |
| Physical and Chemical Properties | Chemical properties colorless oily liquid. The melting point is 50-52 ℃, and the boiling point is 121-123 ℃(0.267kPa). Slightly soluble in water, soluble in ethanol, ether, benzene. |
| Use | Uses intermediates in organic synthesis. |
6-Methoxylepidine - Risk and Safety
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. |
6-Methoxylepidine - Upstream Downstream Industry
| Raw Materials | Ethanol Zinc chloride Ferric chloride p-Anisidine |
| Downstream Products | 6-Methoxyquinoline-4-carbaldehyde |
6-Methoxylepidine - Production method
100g of p-methoxyaniline hydrochloride, 270g of ferric chloride (FeCL3 · 6H2O), 10g of anhydrous zinc chloride and 450ml of 95% ethanol are mixed, stirred and heated, 35g of methyl vinyl ketone is added dropwise, maintained at 60-65 ℃ for 1.5-2h, and refluxed for 2h. After cooling, add 25% sodium hydroxide solution until it is alkaline, and distill under reduced pressure. Then the residue is extracted with ether, the extract is distilled after the ether is distilled, and the fraction at 121-123 ℃(0.267kPa) is collected to obtain 42g of the product with a yield of 52%.
Last Update：2024-04-10 22:29:15
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Product Name: 4-Methyl-6-Methoxyquinoline Visit Supplier Webpage Request for quotation
CAS: 41037-26-7
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CAS: 41037-26-7
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Raw Materials for 6-Methoxylepidine
Downstream Products for 6-Methoxylepidine