production method | the preparation method is to put sodium hydride and toluene in a reaction kettle, under stirring, the mixture of methyl α-chloropropionate and methyl propionate is added dropwise, the reaction is maintained at 20~25 ℃ for several hours, then the stabilizer is added dropwise to promote the completion of the reaction, and then water is added dropwise, after stirring, the mixture was left to stand and layered, the aqueous layer was extracted with toluene, and the toluene layer and the extraction layer were combined to obtain the product after being dissolved. |