69559-11-1
2-(4-Aminopentyl(ethyl)amino)ethanol
CAS: 69559-11-1
Molecular Formula: C9H22N2O
69559-11-1 - Names and Identifiers
69559-11-1 - Physico-chemical Properties
| Molecular Formula | C9H22N2O |
| Molar Mass | 174.28 |
| Density | 0.935 |
| Boling Point | 93 °C(Press: 0.6 Torr) |
| Storage Condition | Room Temprature |
| Refractive Index | 1.47 |
| Physical and Chemical Properties | Colorless and pure liquid. |
| Use | For pharmaceutical applications |
69559-11-1 - Synthesis of 5-(N-ethyl-N-2-Hydroxyethyl amine)-2-pentylamine
from VIP Journal Professional Edition
Author:
residual Dan , Li xiang , Liu Xiaocheng , dunagalun , Liu Xie , Chen Gang
Abstract:
with 5-chloro-2-pentanone as raw material, carbonyl protection was carried out first, deprotection was carried out after reaction with ethyl ethanolamine, and then carbonyl reductive amination was carried out, 5-(N-ethyl-N-2-Hydroxyethyl amine)-2-pentylamine (commonly known as hydroxychloroquine side chain) was synthesized by 4 steps reaction. The total yield was 53.8% and the purity was 99.0%(GC). The recovery rate of ethyl ethanolamine was 95%.
Key words:
5-(N-ethyl-N-2-Hydroxyethyl amine)-2-pentylamine hydroxychloroquine hydroxychloroquine intermediate
DOI:
CNKI:SUN:HBHG.0.2014-05-015
year:
2014
Last Update：2024-01-02 23:10:35
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