916597-01-8 - Names and Identifiers
916597-01-8 - Physico-chemical Properties
916597-01-8 - Introduction
Bis(methylcyclopentadienyl)(methyl)(methoxy)zirconium(IV), often referred to simply as (nr-methylcyclopentadienyl)(methyl)(methoxy)zirconium(IV), is an organic zirconium compound. The following is its nature, use, preparation and safety information:
Nature:
-Appearance: Colorless or light yellow solid.
-Melting point: about 80-100°C.
-Solubility: Soluble in some non-polar organic solvents, such as toluene and benzene.
-Its structure can be verified by nuclear magnetic resonance (NMR) and infrared spectroscopy (FT-IR).
Use:
- (η-methylcyclopentadienyl) (methyl) (methoxy) zirconium (IV) is widely used in the field of organic synthesis, especially as a catalyst precursor in coordination polymerization reactions.
-It can be used to synthesize polyolefins, polymer materials and nanomaterials and other related compounds.
Preparation Method:
- (η≤-methylcyclopentadienyl) (methyl) (methoxy) zirconium (IV) is usually prepared by the following steps:
1. Silver methylcyclopentadienyl [(η„-CpMe)Ag] is reacted with lithium methoxide (LiOMe) to obtain lithium methylcyclopentadienyl (η„-CpMeLi).
2. Methylcyclopentadienyl lithium is reacted with zirconium (IV) chloride to produce the desired target product.
Safety Information:
- (η-Methylcyclopentadienyl) (methyl) (methoxy) zirconium (IV) should follow appropriate safety measures during use, such as wearing protective gloves, glasses and laboratory atmospheric air extraction devices.
-It may react violently to water, so contact with water should be avoided.
-When storing and handling (ηL-methylcyclopentadienyl) (methyl) (methoxy) zirconium (IV), keep the storage container sealed and away from fire and oxidizing agents.
Last Update:2024-04-09 20:49:11