Name | BIS(DIBUTYLAMINO)DISULFIDE |
Synonyms | BIS(DIBUTYLAMINO)DISULFIDE 1-Butanamine, N,N'-dithiobis[N-butyl- |
CAS | 67271-09-4 |
Molecular Formula | C16H36N2S2 |
Molar Mass | 320.6 |
Physical and Chemical Properties | This product is oily liquid, insoluble in water, soluble in xylene, toluene, etc. |
use | bis-n-butylamine disulfide is an intermediate of the synthetic insecticide carbosulfan. |
production method | di-n-butylamine, sodium hydroxide solution and xylene are added into the reaction kettle, sulfur monochloride is added under stirring, the reaction is exothermic, the addition is completed, stirring is carried out for 1h, the oil layer is left to be separated into water layer, and the oil layer is washed with dilute hydrochloric acid and water until neutral for later use. The reaction equation is as follows:(n-C4H4)2NH S2Cl2 →[(n-C4H9)2NS-]2 2HCl |