M-BROMOANISOLE
3-Bromoanisole
CAS: 2398-37-0
Molecular Formula: C7H7BrO
M-BROMOANISOLE - Names and Identifiers
M-BROMOANISOLE - Physico-chemical Properties
| Molecular Formula | C7H7BrO |
| Molar Mass | 187.03 |
| Density | 1.490g/mLat 20°C |
| Melting Point | 2 °C |
| Boling Point | 210-211°C(lit.) |
| Flash Point | 200°F |
| Water Solubility | Miscible in methanol, benzene, hexane, toluene and dichloromethane. Practically insoluble in water. |
| Solubility | DMSO (Sparingly), Methanol (Slightly) |
| Vapor Presure | 38.39Pa at 25℃ |
| Appearance | Liquid |
| Specific Gravity | 1.477 |
| Color | Clear colorless to slightly yellow-brown |
| BRN | 1524687 |
| PH | 5.5 (H2O, 20℃) |
| Storage Condition | Sealed in dry,Room Temperature |
| Stability | Stable. Combustible. Incompatible with strong oxidising agents, strong acids reducing agents. |
| Refractive Index | n20/D 1.563(lit.) |
| Physical and Chemical Properties | Density 1.477 melting point 2°C boiling point 210-211°C refractive index 1.563-1.565 flash point 93°C |
| Use | For Organic synthesis |
M-BROMOANISOLE - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Safety Description | S23 - Do not breathe vapour. S24/25 - Avoid contact with skin and eyes. |
| WGK Germany | 3 |
| FLUKA BRAND F CODES | 8 |
| TSCA | T |
| HS Code | 29093038 |
| Hazard Note | Irritant |
M-BROMOANISOLE - Upstream Downstream Industry
| Raw Materials | Benzene Benzene Methyl alcohol Methyl alcohol Sulfuric acid Sulfuric acid Hydrogen Bromine Sodium bromate Sodium bromate |
| Downstream Products | Tramadol |
M-BROMOANISOLE - Reference Information
| LogP | 3.03 |
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| use | organic synthetic raw materials. Used in organic synthesis It is the main intermediate in the synthesis of anti-cancer, sedative and analgesic Qu Moduo, and can be used in other medicines, dyes and organic synthesis. |
| Production method | It is obtained by the reaction of m-bromophenol and dimethyl sulfate. Dissolve m-bromophenol in sodium hydroxide solution, slowly add dimethyl sulfate dropwise under stirring, heat for 1h, and cool the layered colorless oil. The water layer is extracted with ether, dried, and distilled to recover ether, and the residue and oil are distilled under reduced pressure to obtain the finished product. The yield is 90%. |
Last Update：2024-04-10 22:29:15
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Raw Materials for M-BROMOANISOLE
Downstream Products for M-BROMOANISOLE