N-Boc-(S)-3-morpholine-methanol
(S)-N-Boc-2-Hydroxymethylmorpholine
CAS: 135065-76-8
Molecular Formula: C10H19NO4
N-Boc-(S)-3-morpholine-methanol - Names and Identifiers
N-Boc-(S)-3-morpholine-methanol - Physico-chemical Properties
| Molecular Formula | C10H19NO4 |
| Molar Mass | 217.26 |
| Density | 1.118 |
| Melting Point | 60-62 °C |
| Boling Point | 321 °C |
| Flash Point | 148 °C |
| Water Solubility | Slightly soluble in water. |
| Vapor Presure | 2.53E-05mmHg at 25°C |
| Appearance | White solid |
| pKa | 14.36±0.10(Predicted) |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
| Sensitive | Light Sensitive |
| Refractive Index | 1.474 |
| MDL | MFCD09260606 |
N-Boc-(S)-3-morpholine-methanol - Reference Information
| use | N-tert-butoxycarbonyl-(S)-2-morpholine methanol is a useful research chemical. N-tert-butoxycarbonyl-(S)-2-morpholine methanol is mainly used in medicine and pesticide intermediates. |
| preparation | at 0 ℃, borane (1M,20mL) was dropwise added to the solution of (S)-4-(tert-butoxycarbonyl) morpholine -2-formic acid (2.50g,10.8mmol) in THF(25mL) , for 15min. After adding, warm the reaction mixture to room temperature and stir for 2 small . At 0°C, the reaction mixture was quenched with MeOH/AcOH(9:1,10mL). The mixture was then concentrated and the residue poured into 35mL of water and 35mL EtOAc. The organic layer was washed with a saturated Na2CO3(30mL) aqueous solution, dried with Na2SO4 and concentrated to obtain N-tert-butoxycarbonyl-(S)-2-morpholine methanol (2.6g,100%), which was a colorless oil. |
Last Update：2024-04-10 22:29:15
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