Trichlorotris(tetrahydrofurane)titanium(III)
Titanium(III) chloride tetrahydrofuran complex
CAS: 18039-90-2
Molecular Formula: C12H24Cl3O3Ti
Trichlorotris(tetrahydrofurane)titanium(III) - Names and Identifiers
Trichlorotris(tetrahydrofurane)titanium(III) - Physico-chemical Properties
| Molecular Formula | C12H24Cl3O3Ti |
| Molar Mass | 370.54 |
| Melting Point | 250 °C |
| Appearance | Powder or Crystals |
| Color | Blue to blue-green or |
| Storage Condition | Refrigerator (+4°C) + Flammables area |
| Sensitive | 8: reacts rapidly with moisture, water, protic solvents |
Trichlorotris(tetrahydrofurane)titanium(III) - Risk and Safety
| Hazard Symbols | C - Corrosive F,C,F - |
| Risk Codes | R34 - Causes burns R29 - Contact with water liberates toxic gas R19 - May form explosive peroxides R14 - Reacts violently with water R11 - Highly Flammable |
| Safety Description | S8 - Keep container dry. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S16 - Keep away from sources of ignition. S27 - Take off immediately all contaminated clothing. |
| UN IDs | 2925 |
| HS Code | 29310099 |
Trichlorotris(tetrahydrofurane)titanium(III) - Reference Information
| preparation | The titanium tetrahydro-furan chloride was prepared as follows: to a 2L round-bottom flask (equipped with a thermometer, mechanical stirrer and reflux condenser) particulate titanium (-100 mesh, 99.9 purity, 8.3g), titanium tetrachloride (98.6g) and toluene (g) were added to the solution. THF(432g) was added under ice-cooling while maintaining the pot temperature at 10-20 °c. The reaction mixture was heated to reflux (90-100 °c) for 6 hours. The reaction mixture was then cooled to room temperature and filtered. The solid titanium tetrahydrofuran chloride product was washed with deoxy-hexane (240 ml) and dried under vacuum, yield = 94% grams;, based on the total charge of titanium (TiCl4 and particulate titanium). |
Last Update：2024-04-10 22:29:15
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