Molecular Formula | C14H12N2O2 |
Molar Mass | 240.26 |
Density | 1.1613 (rough estimate) |
Melting Point | >190°C (dec.) |
Boling Point | 382.97°C (rough estimate) |
Appearance | Purple crystal |
Storage Condition | Room Temprature |
Refractive Index | 1.618 |
Physical and Chemical Properties | Deep purple needle crystals (in pyridine) or purple crystals. Soluble in benzene, pyridine, nitrobenzene, aniline, slightly soluble in hot acetic acid, ethanol. |
Use | Use 1, 4-diaminoanthraquinone leucosomes are anthraquinone-derived dyes that are mixed products produced by the combustion of a mixture of red and purple smoke. |
patent for invention
application (patent) number:
CN201810800333.0
date of application:
20180720
public/announcement number:
CN109096120A
date of publication/announcement:
20181228
Applicant (patentee):
Jiangsu Wale Chemical Co., Ltd
Inventor:
national and provincial code:
CN320724
Summary:
The present invention discloses a preparation process of a mixture of 1,4 diaminoanthraquinone leuco and an oxide, which belongs to the field of organic synthesis and includes the following steps: adding 1,4 dihydroxyanthraquinone, sodium sulfite, 15 ~ 20wt% ammonia solution, airtight container, stirring for more than 0.5 hours, then slowly heating to 90~95 ℃, keeping the temperature for 4~6 hours, cooling and pressure, reduce to 30~35 degrees Celsius, filter, wash until the washing water is neutral, discharge and dry to obtain the product. The process described in the present invention reduces the amount of insurance powder and the amount of oxidant used in the subsequent product process.
202120777494
Applicant (patentee):
hunan institute of humanities science and technology
Inventor:
Peng Weicai ,< a href = "https://xueshu.baidu.com/s?wd=author: (Wei Congcong) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Wei Congcong ,< a href = "https://xueshu.baidu.com/s?wd=author: (Liu Changhong) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Liu Changhong , Liu Qiaolin , Qin Fei ,< a href = "https://xueshu.baidu.com/s?wd=author: (Li Wei) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Li Wei ,< a href = "https://xueshu.baidu.com/s?wd=author: (Wen Jin) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Wen Jin ,< a href = "https://xueshu.baidu.com/s?wd=author: (Peng Yangxi) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Peng Yangxi ,< a href = "https://xueshu.baidu.com/s?wd=author: (Guo Jun) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Guo Jun
patent for invention
application (patent) number:
CN201911325649.X
date of application:
20191220
public/announcement number:
CN111087314A
date of publication/announcement:
20200501
Applicant (patentee):
Nanjing jinhao pharmaceutical technology co., ltd
Inventor:
Wu Jianzhong ,< a href = "https://xueshu.baidu.com/s?wd=author: (Zou Xiaodong) & tn = SE_baiduxueshu_c1gjeupa & ie = utf-8 & SC _f_para = SC _hilight = person" target = "_blank"> Zou Xiaodong
national and provincial code:
CN320100
Summary:
the invention discloses a synthesis method of 1,4 diaminoanthraquinone and its leuco, adding 1,4 dihydroxyanthraquinone, sodium hydroxide, sodium hydrosulfite and ammonia solution to a high-pressure reaction kettle, sealing the autoclave, stirring evenly, heating to 8595 ℃, holding the reaction for several hours, then cooling to 4050 ℃, discharging the material under pressure, washing with hot water to PH 78, and drying. The invention adds sodium hydroxide and sodium hydroxide when feeding, so as to give full play to the reducing effect of the sodium hydroxide. While improving product quality, it reduces the cost pressure caused by the treatment of three wastes. The purity of the obtained 1,4 diaminoanthraquinone and its leuco products is increased from 90% to 95%, the yield is increased from 80% to 88%, and the obtained ammonia nitrogen wastewater is halved, which reduces the cost of ammonia nitrogen wastewater; this process does not use organic solvents, while reducing the use of ammonia water, reducing the cost of recycling and processing organic solvents.