Molecular Formula | C6H8Cl2O5 |
Molar Mass | 231.03 |
Density | 1.5876 (rough estimate) |
Boling Point | 330.45°C (rough estimate) |
Flash Point | 99 °C |
Storage Condition | Room Temprature |
Refractive Index | 1.53 |
Safety Description | S16 - Keep away from sources of ignition. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S27 - Take off immediately all contaminated clothing. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S61 - Avoid release to the environment. Refer to special instructions / safety data sheets. S23 - Do not breathe vapour. S60 - This material and its container must be disposed of as hazardous waste. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. |
UN IDs | 2742 |
Abstract:
In the phosgene synthesis of diethylene glycol bis-chloroformate, diethylene glycol can be added dropwise in the liquid light by dropwise addition. After synthesizing diethylene glycol bis-chloroformic acid ester, the finished product should be obtained by driving light with nitrogen; however, for the traditional diethylene glycol bischloroformate production process, because it is not easy to control the color of the product, it will affect the production quality of the product. Therefore, it should be improved with the improvement measures to optimize the synthesis process, to improve the synthesis quality of diethylene glycol bischloroformate. The following analysis of diethylene glycol bischloroformate phosgene synthesis experiment.
Key words:
phosgene synthesis diethylene glycol bischloroformate experiment
DOI:
10.3969/j.issn.1674-5167.2015.04.146
year:
2015
CN201811595662.2
application date:
2018-12-25
Public/Announcement Number:
CN109721494A
Public/announcement date:
2019.05.07
applicant (patent):
Hangzhou more blue Biotechnology Co., Ltd.
inventor:
National and provincial code:
CN330108
Abstract:
The invention relates to a method for synthesizing diethylene glycol dichloride, which uses dichloromethane as an extractant and uses a decanter for extraction, which can effectively improve the extraction and separation efficiency, reduce the amount of extractant and process water, the obtained nitrate and chlorine liquid purity is good, can be directly used in the next step reaction, the concentration of waste sulfuric acid obtained relative to the water analysis method is high, can be directly used in the preparation of ferrous sulfate and other processes.