Molecular Formula | C10H20O2 |
Molar Mass | 172.26 |
Density | 0.9516 g/cm3 |
Boling Point | 93-95 °C(Press: 3 Torr) |
Water Solubility | 23g/L at 23℃ |
Vapor Presure | 1Pa at 20℃ |
pKa | 14.69±0.40(Predicted) |
CN201410671128.0
application date:
2014-11-21
Public/Announcement Number:
CN104370867B
Public/announcement date:
2017.03.15
applicant (patent):
Shandong Xincheng Pharmaceutical Co., Ltd.
inventor:
Zhang Jinzhong , horse call , Li Junsheng , Fang Wanjun , Hu shuitao , anvern , Ma Xiao , Jia Huiming , Zhu Quantong
National and provincial code:
CN370703
Abstract:
The invention discloses a preparation method of perfume 4 methyl 2(2 methyl propyl) 2h Tetrahydropyran 4 alcohol, which comprises the following steps: preparation of hydroxy rose ether and hydrogenation reaction; the step of preparing hydroxy rose ether comprises the steps of adding raw material and catalyst, heating up and adding another raw material, reacting and filtering; The step of hydrogenation reaction comprises the steps of adding raw material and catalyst, nitrogen hydrogen replacement, reaction, filtration, purification steps. Reaction using solid acid as a catalyst, will not produce waste acid water, waste alkali water, etc., to reduce environmental pollution; Intermediate hydroxy rose ether as a solid, easy to purify; After hydrogenation, the product purity is high, the product aroma is good; the purity of the product prepared by this method is more than 99.2%.
LogP | 1.65 at 23℃ |
EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |