Molecular Formula | C3Cl6 |
Molar Mass | 248.75 |
Density | 1.765 g/mL at 25 °C(lit.) |
Melting Point | -73°C |
Boling Point | 209-210 °C(lit.) |
Flash Point | 209-210°C |
Water Solubility | Insoluble in water. |
Solubility | Acetonitrile (Slightly), Chloroform (Sparingly), Methanol (Slightly) |
Vapor Density | 8.3 (vs air) |
Appearance | Morphological Oil |
Color | Colourless |
BRN | 1766640 |
Storage Condition | Refrigerator, Under inert atmosphere |
Stability | Stable. Incompatible with strong oxidizing agents. |
Refractive Index | n20/D 1.549(lit.) |
MDL | MFCD00000835 |
Physical and Chemical Properties | Chemical colorless liquid. Boiling point 209-210 ℃,99 ℃(1.33kPa), relative density 1.765, refractive index 1.5490(20 ℃), insoluble in water. |
Use | Uses for organic synthesis. |
Hazard Symbols | T - Toxic |
Risk Codes | R23 - Toxic by inhalation R36/37/38 - Irritating to eyes, respiratory system and skin. |
Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) |
UN IDs | UN 3382 6.1/PG 1 |
WGK Germany | 3 |
RTECS | UD0175000 |
FLUKA BRAND F CODES | 19 |
TSCA | Yes |
Hazard Class | 6.1 |
Packing Group | III |
Raw Materials | Potassium ethylate 1,1,1,2,2,3,3-HEPTACHLOROPROPANE |
toxic substance data | 1888-71-7(Hazardous Substances Data) |
EPA chemical information | Hexachloropropene (1888-71-7) |
Dissolve 1,1,1,2,3, 3-heptachloropropane in ethanol, keep it at 30-40°C, add potassium ethoxide solution dropwise, and then heat and reflux for 1h. The ethanol in the reactant is evaporated and recovered, cooled and poured into water for stratification, the organic layer is washed with water, dried, distilled under reduced pressure, and the fraction at 98-100 ℃(2.67kPa) is collected to obtain hexachloropropene with a yield of 86.7-89.2.