36075-68-0
4-BROMO-8-METHYLQUINOLINE
CAS: 36075-68-0
Molecular Formula: C10H8BrN
36075-68-0 - Names and Identifiers
| Name | 4-BROMO-8-METHYLQUINOLINE |
| Synonyms | 4-BROMO-8-METHYLQUINOLINE Quinoline, 4-bromo-8-methyl- |
| CAS | 36075-68-0 |
36075-68-0 - Physico-chemical Properties
| Molecular Formula | C10H8BrN |
| Molar Mass | 222.08 |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
36075-68-0 - Reference Information
| Introduction | 4-bromo-8-methylquinoline is a pharmaceutical intermediate, which can be obtained by bromination of 8-methylquinoline-4-ol and phosphorus tribromide. It has been reported that it can be used to prepare pyranopyrazoles and pyrazolopyridines immunomodulators for the treatment of autoimmune diseases. |
| application | 4-bromo -8-methylquinoline can be used as an organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process. |
| preparation | 8-methylquinoline -4-alcohol (500mg,3.14mmol,1.00 equivalent) and N,N-dimethylformamide (20mL) were added to a 100mL round bottom flask. Then phosphorus tribromide (851 mg,3.14mmol,1.20 equivalent) was added drop by drop under room temperature stirring, and the obtained solution was stirred at room temperature for 15 hours. Then add water/ice (100mL) to quench the reaction. Use sodium hydroxide (2mol/L) to adjust the pH of the solution to 10. The solids were collected by filtration to obtain 660mg(95%) of 4-bromo-8-methylquinoline, which was a light yellow solid. |
Last Update：2024-04-09 20:49:11
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View History
36075-68-0
2160-93-2
436799-33-6
Fexofenadine
175204-90-7
(2-hydroxyethyl)ammonium
CS-820
PHENYL FORMATE
分散黄GHS
2160-93-2
436799-33-6
Fexofenadine
175204-90-7
(2-hydroxyethyl)ammonium
CS-820
PHENYL FORMATE
分散黄GHS