ANILINE-D7
ANILINE-D7
CAS: 14545-23-4
Molecular Formula: C6D7N
ANILINE-D7 - Names and Identifiers
ANILINE-D7 - Physico-chemical Properties
| Molecular Formula | C6D7N |
| Molar Mass | 100.17 |
| Density | 1.098g/mLat 25°C |
| Melting Point | -6°C(lit.) |
| Boling Point | 184°C(lit.) |
| Flash Point | 158°F |
| Storage Condition | 2-8°C |
| Stability | Stable, but light sensitive. May discolour upon exposure to air or light. Incompatible with oxidizing agents, bases, iron, iron salts, aluminium, zinc. |
| Refractive Index | n20/D 1.5824(lit.) |
| Physical and Chemical Properties | EPA Chemical Information Aniline-d7 (14545-23-4) |
ANILINE-D7 - Risk and Safety
| Risk Codes | R20/21/22 - Harmful by inhalation, in contact with skin and if swallowed. R40 - Limited evidence of a carcinogenic effect R48/23/24/25 - R50 - Very Toxic to aquatic organisms R68 - Possible risk of irreversible effects R43 - May cause sensitization by skin contact R41 - Risk of serious damage to eyes R23/24/25 - Toxic by inhalation, in contact with skin and if swallowed. |
| Safety Description | S28 - After contact with skin, wash immediately with plenty of soap-suds. S36/37 - Wear suitable protective clothing and gloves. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S61 - Avoid release to the environment. Refer to special instructions / safety data sheets. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S63 - S46 - If swallowed, seek medical advice immediately and show this container or label. S27 - Take off immediately all contaminated clothing. |
| UN IDs | UN 1547 6.1/PG 2 |
| WGK Germany | 3 |
| HS Code | 28459000 |
ANILINE-D7 - Upstream Downstream Industry
| Downstream Products | ANILINE D5 |
ANILINE-D7 - Reference Information
| preparation | deuterated aniline is prepared as follows: aniline 10mmol, heavy water 20mL and SOCl20.3 mL are sequentially added to the reaction bottle for 24 hours of reflux reaction. Cooling to room temperature, TLC detection reaction is complete [developing agent: A = V (ethyl acetate):V (petroleum ether) = 1: 10], adjusted to pH7 with saturated sodium bicarbonate solution, extracted with ethyl acetate (3 × 20mL), combined with organic layers, washed with saturated salt water (2 × 15mL), dried with anhydrous Na2SO4, filtered, concentrated filtrate and then processed by silica gel column chromatography (eluent: A = 1 ∶ 20) purified deuterated aniline. |
| EPA chemical information | information provided by: ofmpub.epa.gov (external link) |
Last Update：2024-04-10 22:29:15
ANILINE-D7 - Preparation
deuterated aniline was prepared as follows: 10mmol of aniline, 20mL of heavy water and 20.3mL of SOCl20 were added to the reaction bottle in sequence, and the reaction was refluxed for 24 hours. Cooling to room temperature, TLC detection reaction is complete [developing agent: A = V (ethyl acetate):V (petroleum ether) = 1: 10], adjusted to pH7 with saturated sodium bicarbonate solution, extracted with ethyl acetate (3 × 20mL), combined with organic layers, washed with saturated salt water (2 × 15mL: A = 1 ∶ 20) purified deuterated aniline.
Last Update：2024-04-10 22:29:15
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Product Name: Benzen-2,3,4,5,6-d5-amine-d2 Visit Supplier Webpage Request for quotationCAS: 14545-23-4
Tel: +86-400-900-4166
Email: product@acmec-e.com
Mobile: +86-18621343501
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Multiple Specifications
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Downstream Products for ANILINE-D7