12222-78-5
Disperse Blue BGL
CAS: 12222-78-5
Molecular Formula: C20H14N2O5
12222-78-5 - Names and Identifiers
12222-78-5 - Physico-chemical Properties
| Molecular Formula | C20H14N2O5 |
| Molar Mass | 362.09 |
| Storage Condition | Room Temprature |
| Physical and Chemical Properties | Chemical Properties Disperse Blue BGL is a blue powder, soluble in acetone and ethanol. The color light of copper and iron ions changes during dyeing. |
| Use | Uses Disperse Blue BGL is mainly used for dyeing polyester and its blended fabrics, and also used for dyeing acetate fiber, triacetate fiber and nylon. Suitable for high temperature and high pressure method, hot melt method and carrier method of dyeing. The color is brilliant blue, the fastness is excellent, has excellent color matching performance, often with disperse Yellow Brown 2RFL, disperse Red Jade 2GFL combination dyeing a variety of light, medium and dark colors. The polyester/cotton blended fabric can be dyed with reactive dyes in the same bath. |
12222-78-5 - Nature
| EPA chemical information | C. I. Disperse Blue 73 (12222-78-5) |
Last Update：2024-04-10 22:29:15
12222-78-5 - Uses and synthesis methods
introduction
disperse blue BGL, blue powder, is formed by sulfonation, nitration and reduction of 1,5-dicarboxyl A,8-hydrocyan -2.6-sodium disulfonate from 1,5-shuttle onion, and then in the presence of boric acid and sulfuric acid, it is added with phenol and anisole, transposition and desulphurization. Dispersed blue BGL is used for printing and dyeing polyester and its blended fabrics, and has good color matching performance with yellow brown 2HFL and red jade 2GFL.
production method
Using 1, 5-dihydroxyanthraquinone, phenol, and this methyl ether as raw materials, first sulfonate, nitrate, and reduce 1, 5-dihydroxyanthraquinone to obtain 1, 5-dihydroxy-4, 8-Diaminoanthraquinone -2, 6-disulfonate sodium, and then add it with phenol and anisole respectively, and finally hydrolyze the sulfonic acid group to obtain the product. After filtration, water washing to neutral, grinding, drying to obtain the finished product..
1 part of 1,5-dihydroxyanthraquinone, 13.98 parts of fuming sulfuric acid and 0.53 parts of anhydrous sodium sulfate were sulfonated at 110-115 ℃ for 4 hours and diluted with 6.92 parts of sulfuric acid. The sulfonated dilution is mixed with the prepared mixed acid [prepared from 4.73kg of nitric acid (95%), 9.7kg of sulfuric acid (96%) and 1.9kg of water], heated to 55-60 ℃ for nitrification, cooled and filtered. Take 47.2kg of nitrification filter cake and 8.25kg of sodium sulfide (100%), carry out reduction reaction at 75-78 ℃ for 1.5-2h, press filtration, wash with salt and alkali solution until there is no sodium sulfide, and obtain 1,5-dihydroxy -4,8-diaminoanthraquinone -2,6-disulfonate sodium (I).
take 1 part (I), 1.2 parts anisole, 31 parts sulfuric acid, 2.34 parts boric acid and 82kg of ice water, carry out addition reaction at 12 ℃ 2 ℃ for 1h, dilute with water, translocation at (95±3)℃, and keep warm for 3h. Then add 8.2kg of table salt, filter, and wash with 2% salt water until neutral. Take 1 part of the indexed product filter cake, 34kg of ammonia water (35%) and 0.99 parts of sodium hydrosulfonic acid group hydrolysis reaction at 60-70 ℃, the reaction is finished, filtered, washed with hot water until neutral, and the filter cake is mixed with 2 parts of diffusion agent to obtain A component dye.
synthesize component B dye and replace anisole with 2.55 parts of phenol. The translocation reaction was carried out at 90 ℃ 2 ℃ for 3h. The rest is the same as the synthetic A component. A component dye and B component dye are mixed in a certain proportion to obtain the finished product.
Last Update：2024-04-10 22:29:15
Supplier List
Spot supply
Product Name: Disperse Blue BGL Request for quotationCAS: 12222-78-5
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3787852685
Spot supply
Product Name: Disperse Blue BGL Request for quotationCAS: 12222-78-5
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3785839865
Product Name: Disperse Blue BGL Visit Supplier Webpage Request for quotation
CAS: 12222-78-5
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
CAS: 12222-78-5
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
Spot supply
Product Name: Disperse Blue BGL Request for quotationCAS: 12222-78-5
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3787852685
Spot supply
Product Name: Disperse Blue BGL Request for quotationCAS: 12222-78-5
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3785839865
Product Name: Disperse Blue BGL Visit Supplier Webpage Request for quotation
CAS: 12222-78-5
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
CAS: 12222-78-5
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
View History