Molecular Formula | C13H7BrClF3N2 |
Molar Mass | 363.56 |
Physical and Chemical Properties | The chemical product is a white solid, m.p.129 ~ 130 ℃, insoluble in water. |
Use | Use of this product is an intermediate of the insecticide acarene. |
The preparation method is obtained by bromination of 2-p-chlorophenyl-1-methyl-5-trifluoromethylpyrrole -3-nitrile.
6.1g(0.02mol)2-p-chlorophenyl -1-methyl -5-trifluoromethyl pyrrole -3-nitrile, 6.4g(0.03mol) bromine and 50mL carbon tetrachloride were added to the three-mouth flask respectively, stirred, heated, refluxed for 8-12h, cooled to room temperature, diluted with water, extracted with ethyl acetate, the extract was washed with sodium metabisulfite, recrystallization with n-heptane gave 6.8g of 2-p-chlorophenyl -4-bromo -1-methyl -5-trifluoromethyl pyrrole -3-nitrile with 90% yield.