2-苯甲酰乙酰苯胺
Benzoylacetoanilide
CAS: 959-66-0
Molecular Formula: C15H13NO2
2-苯甲酰乙酰苯胺 - Names and Identifiers
| Name | Benzoylacetoanilide |
| Synonyms | AKOS BBS-00000685 Benzoylacetoanilide 2-Benzoylacetanilide 2-BENZOYLACETANILIDE 2-BENZOYLACETOANILIDE 3-oxo-3-phenylpropionanilide 2-Benzoylacetoanilide(alpha-] 3-oxo-N,3-diphenylpropanamide N,3-Diphenyl-3-oxopropionamide N-Phenyl-β-oxobenzenepropanamide |
| CAS | 959-66-0 |
| EINECS | 213-503-7 |
| InChI | InChI=1/C15H13NO2/c17-14(12-7-3-1-4-8-12)11-15(18)16-13-9-5-2-6-10-13/h1-10H,11H2,(H,16,18) |
| InChIKey | XRZDIHADHZSFBB-UHFFFAOYSA-N |
2-苯甲酰乙酰苯胺 - Physico-chemical Properties
| Molecular Formula | C15H13NO2 |
| Molar Mass | 239.27 |
| Density | 1.205±0.06 g/cm3(Predicted) |
| Melting Point | 106-108 °C (lit.) |
| Boling Point | 473.6±28.0 °C(Predicted) |
| Flash Point | 194.5°C |
| Solubility | acetone: soluble25mg/mL, clear, colorless to faintly yellow |
| Vapor Presure | 3.9E-09mmHg at 25°C |
| Appearance | powder to crystal |
| Color | White to Almost white |
| pKa | 11.37±0.23(Predicted) |
| Refractive Index | 1.624 |
2-苯甲酰乙酰苯胺 - Risk and Safety
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. |
| WGK Germany | 2 |
| RTECS | AB4542950 |
2-苯甲酰乙酰苯胺 - Reference Information
| properties | acetanilide, also known as N-phenylacetamide, acetamidobenzene, commonly known as cooling ice. Those crystallized from water are orthogonal strains of white scale-like glossy crystals or white crystalline powder. |
| Application | 2-benzoylacetanilide is a very versatile acylating agent in organic synthesis, it can also be used as intermediates and Analytical reagents for pesticides. Although benzoyl acetanilide has applications, but the domestic literature on the synthesis of 2-benzoyl Acetanilide is rarely reported, so the study on the preparation method of 2-benzoyl acetanilide has important industrial application value. |
| Use | Acetanilide can be used as a raw material for veterinary medicine (including fish), for the preparation of intermediate chloroacetanilide and p-aminobenzenesulfonamide, further production of "sulfadimethoxy pyrimidine", "sulfadiazine methoxy pyrimidine", "sulfamethoxyl pyridazine", "sulfathiazole", "sulfamethazine", "sulfamethoxine thiazole" and other drugs. |
| preparation | in a 250mL four-necked flask equipped with a thermometer, add 40g of petroleum ether, 19.2g of ethyl benzoyl acetate, 11.2g of aniline, the catalyst is 0.5g, the condenser tube is installed, and the stirrer is turned on. When the temperature is raised to 120-130 ° C., the ethanol is continuously distilled during the reaction, and the reaction time is 6-12H. After the reaction is finished, filtering is carried out, and the filtered organic phase is cooled to 8-10 ° C., the crystallization is complete, and the benzoyl acetanilide product is obtained by centrifugal filtration. The yield of the product is 94.92%, and the melting point is 107-108 ° C. |
Last Update：2024-04-10 22:29:15
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Product Name: 2-Benzoylacetanilide Visit Supplier Webpage Request for quotationCAS: 959-66-0
Tel: +86-400-900-4166
Email: product@acmec-e.com
Mobile: +86-18621343501
QQ: 2881950922
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Product Name: 2-Benzoylacetanilide Visit Supplier Webpage Request for quotationCAS: 959-66-0
Tel: +86-18821248368
Email: Int06@meryer.com
Mobile: +86-18821248368
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View History
2-苯甲酰乙酰苯胺
2-碘苯甲酸叔丁酯
R(-)-PROPYLNORAPOMORPHINE HCL
(二乙胺基)二甲基硅烷
四正丁基氢氧化
N-苯甲酰基-5'-O-[二(4-甲氧基苯基)苯基甲基]-2'-O-(2-甲氧基乙基)-5-甲基胞苷 3'-[2-氰基乙基 N,N-二异丙基氨基亚磷酸酯]
二烯丙基丙二酸二甲酯
2-碘苯甲酸叔丁酯
R(-)-PROPYLNORAPOMORPHINE HCL
(二乙胺基)二甲基硅烷
四正丁基氢氧化
N-苯甲酰基-5'-O-[二(4-甲氧基苯基)苯基甲基]-2'-O-(2-甲氧基乙基)-5-甲基胞苷 3'-[2-氰基乙基 N,N-二异丙基氨基亚磷酸酯]
二烯丙基丙二酸二甲酯